Sep 142009
You start off by making absolutely pure anhydrous hydrogen azide, which is a proposal that you don’t hear very often around the lab, and is the sort of thing that leads to thoughts of career changes. (Maybe I could go into the insurance business and sell policies to whoever took over the prep). The next step is introduction of the fluorine, and when elemental fluorine is the most easily handled reagent in your scheme, let me tell you, you’re in pretty deep.
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